Making X- Distillation and Vaccumes

Well for MDMA reasons to not making it.

1.Safrole oil is very expensive. So is MDP2P(PMK)
2.Glassware, heating mantels, mixers and other equipment is very expensive
3.Chemical are being watched and difficult to buy and very expensive
4.It is time consuming and very exact work
5.It is illegal and you risk going to jail

 

why not just evaporate those other elements by boiling the solution only to the point that the disposable elements evaporate into a flask and dispose of them. then you have only the element you want left, and you don't need to do any more distillation? assuming you have a pure sample.

 

Their are many recepies on the net.
Usually they extract with DCM and then two layers will form because they have different polarities. Like water and oil.
Some procedures just distillate and extract in the purification steps.
Just read the recepies and you will know what to do

 

IS THIS GUY FOR REAL?
My question is this:
CAN A FRACTIONAL DISTILLATION BE DONE WITH SIMPLY ROOTBARK AND WATER UNDER A VACUUM, OR DO YOU FIRST HAVE TO DISTILL THE OIL, AND THEN FRACTIONALLY DISTILL OUT THE SAFROLE? HAS ANYONE EVER TRIED THIS METHOD? DOES THE OIL COME OVER AT THE SAME TEMP. OR DOES JUST THE SAFROLE COME OVER? I WOULD THINK THAT IT WOULD BE ABSOLUTLY NECESSARRY TO DO IT UNDER VACUUM, BUT AM NOT TOO SURE? AND LASTLY, WOULD IT BE PREFERRED TO USE POWDERED ROOT BARK FOR MAXIMUM SURFACE AREA COVERAGE? YOUR EXPERTISE WOULD BE GREATLY APPRECIATED.

BEN dOVER.

 

You need to get the oil out of the bark first (think steam distillation), then fractionally distill the oil (after separating it from the condensate) under vacuum to get the safrole.

If you tried just vacuum distilling a mixture of water and plant matter, all the water would come over, leaving the goods behind.

 

Thanks. It's all becoming a little more clear, although not HALF AS CLEAR apparently as the kid who started this thread. Poor Fucker!


BEN dOVER.

 

How much sassafrass do you need to get enough saffrole for one dose...
And can you just drink the essential oil and get high?

 

its vacuum

 

buy a chemistry book.