Freeze precipitate issues

Discussion in 'DMT' started by MisterWhy, May 11, 2011.

  1. MisterWhy

    MisterWhy Guest

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    Hey all,

    Im a couple of hours away from the last stages of extraction as per SpiceyCat's method. 100g of MMHRB used. After following all instructins my DMT has been in naptha for the past 48 hours in the freezer. Ive just checked and it there is some lovely looking white crystals in there. They seem to be swishing around the bottom of the glass jar. There is another substance stuck to a groove around the bottom of the jar, this is a slightly off white colour. Overall however, there is not a lot of substance or final product.

    Should i freeze precipitate for longer or will this be all the dmt i will get.

    thanks :)
     
  2. Ancient One

    Ancient One Member

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    Did you evap by at least half of volume before freezing?
     
  3. MisterWhy

    MisterWhy Guest

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    Yes, by the time it went in the freezer there was approx 100-150ml or more in a jam jar. This was after 5 pulls. Collected in one container and evap'd in a large pyrex dish before being put back in to a jam jar for freezing.
     
  4. Ancient One

    Ancient One Member

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    Evapping more would've sped things up, leave it in freezer a week; crystals will slowly continue to form...
     
  5. MisterWhy

    MisterWhy Guest

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    Ah ok, am i right in thinking that the naptha will continue to evap even though the lid is on? And that there is still a lot more dmt in the naptha yet to come out?
     
  6. Ancient One

    Ancient One Member

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    Nothing will evap with the lid on....
     
  7. MisterWhy

    MisterWhy Guest

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    Good point......well presented ;) Will give it a little while longer. Thanks bud!
     
  8. jammon

    jammon Member

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    Hope you return from DMT hyperspace
     
  9. jammon

    jammon Member

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    fucking fell in love with dimitri
     
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