so acetone is a good recrystallizing solvent, eh... I figured Et2O would work well too.
representative sample (6 drops from 100 ml solution, 26 drops per ml): [img][img]
two of the best pieces of advice you'll ever get for the A/B extraction: 1) buy a pH meter, you'll be glad you did. Hanna makes a pocket model...
what a jerk; he should be shot in the face. gotta use glass when dealing with aromatic solvents or ketones and he's got a bubbly squarepusher...
to do a MS test , it would have to be from assay (they'd need to have it in a database)
yeah, it would be best to use a ice cold water-cooled condenser, since the vapor pressure of ether is ridiculous; this will ensure you get a nice...
hell yeah. mesc is such a special thing; and since it's not the most economical (profit-wise) drug out there, it is untainted by black market,...
wow... so this is what it looks like in HCL form, after you wash the crap out of it, and recrystallize...
no smoke, you got it. it's a safe route to use the more accesible weak acids and household ammonia, especially for people who haven't done many...
auto starting fluid; you'd need to distill (very carefully) off the ether from the heptane
yezzir
np, lotus. come to think of it, C123, that procedure on drugs-forum isn't half bad. I've noticed that dry powder really balloons up after adding...
man...I don't have the book; my friend does, so I'll have to take a look at it tomorrow when he comes over. steam distillation would be nice,...
synthesis reactions seldom give 100% yields. since this is a base catalyzed hydrolysis reaction, the pH will have to be closely monitored, to...
^ Szara, 1955. it is speculative, as dmt hasn't (yet) been shown to be produced in vivo, yet it has been shown to bind to TA receptors. and...
1) pH of 3 should be fine 2) as many as you feel necessary, probably 3 or 4.. after 5 washings may be pointless though 3) even if the pH is...
yesh. this is where solubility in a particular solvent is really important. chloroform would probably work best (ethanol, or everclear, if it's...
well, the alkaloids won't evaporate, per se, but they will degrade if you keep them in basic solution for too long. and you don't have to be very...
yeah, I went back and saw that (acidification step); I used a 25 drop 32% hcl in 500ml water solution, and did multiple washes on the xylene...
you know what, f#ck it. i'm just gonna skip the defatting, and recrystallize proper at the end. I can see where it's a pain in the ass, working...
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